Nowadays high frequency electronics uses two distinct families of semiconductors-based transistors: field effect transistors and heterojunction bipolar transistors (HBTs). They compete reaching impressive cut off frequencies going up to THz range. Except their usual functions related to switching and amplifying of current or voltage both have been demonstrated as efficient direct THz radiation detectors. Indeed, both types of the transistors have shown that once equipped with antennas, they can capture THz radiation from the open space and deliver the voltage/current proportional to incoming THz radiation power (THz rectification).Most of the work was dedicated to the field effect transistors that rectify THz radiation by plasma related nonlinearities. After pioneering work of [1-2] only very small attention was devoted to HBTs. In this work, we present experimental studies of THz detection by different HBTs fabricated using InP double HBT (DHBT) technologies [3]. Different devices were investigated: single-finger devices and multi-finger devices formed using equally spaced parallel single-transistor fingers [4]. We have evaluated the room temperature detection performances of the devices in the sub-THz range from 250 GHz up to 650 GHz and analyse in details the physical mechanisms of THz detection. Finally, THz domain is an excellent non-contact probe of water content in biological tissues [5]. We also show that the sensitive HBTs detectors can be used for THz spectroscopy and 2D THz imaging to study the water dynamics of sorghum (a grass species cultivated for its grain) by monitoring the dehydration kinetics of its leaves.

Water movement and diffusion in wood is a well-documented research topic. It is strongly linked to the physical and mechanical properties of wood, and thus it has a high degree of importance and prominence for real-life application, particularly in wood drying. Here we employed the terahertz (THz) spectroscopy and imaging techniques to study the diffusion of water in wood. For our first experiments, we used balsa, a species of wood with a relatively homogenous structure (at the tissue level) and a low density that turns into fast diffusion rates and low absorption of the terahertz beam. This enables us to conduct several consecutive observations from various conditions (angles, diffusion directions, etc.) in a short time. These preliminary studies confirm the feasibility of terahertz spectroscopy and imaging techniques as a tool to observe the water diffusion in wood as a function of the direction (Fig. 1). We have also measured the evolution of the attenuation coefficient of the terahertz beam on wet and drying wood at different times. A model of the diffusion behavior based on these measurements, and according to the water content, will be developed and compared with other conventional water diffusion models based on gravimetry methods for the identification of the diffusion coefficients.

Since 2008, epitaxial graphene growth has been developed in terms of homogeneity and scale by using a 1 ATM argon pressure at high temperature (>1650°C). Until now, it still remains challenging to obtain films with different and controlled characteristics such as the thickness or the doping by tuning the growth parameters. Here, we optimized the epitaxial growth of monolayer graphene (1LG) on 4H-SiC (0001) under a low argon pressure of 10 mbar. This intermediate pressure allows growing a continued 1LG in a short process ~1h30.First, we discuss the initial growth stages from buffer layer to 1LG as a function of annealing temperature (same heating rate). The combined Raman spectroscopy and atomic force microscopy analyses show that a buffer layer, fully covering the Si-face of SiC, forms as the first step of growth. Subsequently, 1LG starts to grow at step edges and continue to cover the buffer layer on terraces with a step-flow growth mechanism. Eventually, reproducible syntheses of 1LG films were achieved by this temperature-controlled growth process. Then, we investigate the structural and electronic properties of the 1LG films. The integrated intensity of G-band in Raman spectra normalized with respect to a HOPG reference, AG/AG-HOPG, of each spectrum in Raman map of our continued graphene film is very close to the experimental value reported for a 1LG, demonstrating the good homogeneity. Atomically resolved scanning tunnellingmicroscopy (STM) evidences a (6x6) superstructure, indicative of 1LG covering a reconstructed interface layer[7]. Regarding the transport measurement, quantum Hall plateau values observed in our graphene layers confirmed both continuity and thickness of the1LG film. Moreover, we estimated a hole concentration of p~10^10 - 10^11 /(cm^2) at 1.7 K in helium atmosphere. We ascribe this unusual doping type to an atmosphere contamination effect since we regain the typical n-doped graphene under vacuum by transport measurement and STM analysis.

Since 2008, epitaxial graphene growth has been developed in terms of homogeneity and scale by using a 1 ATM argon pressure at high temperature (>1650°C). Until now, it still remains challenging to obtain films with different and controlled characteristics such as the number of graphene layers or the doping by tuning the growth parameters. Here, we optimized the epitaxial growth of monolayer graphene (1LG) on 4H-SiC (0001) under a low argon pressure of 10 mbar. This intermediate pressure allows growing a continued 1LG in a short process time ~1h30. First, we discuss the initial growth stages from buffer layer (BL) to 1LG as a function of annealing temperature (same heating rate). The combined Raman spectroscopy and atomic force microscopy analyses show that a BL, fully covering the Si-face of SiC, forms as the first step of growth. Subsequently, 1LG starts to grow at step edges and continue to cover the terraces with a step-flow growth mechanism, as demonstrated. Eventually, reproducible syntheses of 1LG films were achieved by this temperature-controlled growth process. Then, we investigate the structural and electronic properties of the 1LG films. The integrated intensity of G-band in Raman spectra normalized with respect to a HOPG reference, AG/AG-HOPG, of each spectrum in Raman map of our continued graphene film is very close to the experimental value reported for a 1LG, demonstrating the good homogeneity. Atomically resolved scanning tunnelling microscopy (STM) evidences a (6x6) superstructure, indicative of 1LG covering a reconstructed interface layer. Regarding the transport measurement, quantum Hall plateau values observed in our graphene layers confirmed both continuity and thickness of the 1LG film8. Moreover, we estimated by transport measurement and STM analysis a hole concentration of pHall~10^10 - 10^11 cm^-2 at 1.7 K in helium atmosphere. We ascribe this unusual doping type to an atmosphere contamination effect since we regain the typical n-doped graphene under vacuum.